TA Instruments

AR1756-0001f

15/03/2013 14:43:45

Sample name	ASW Blank coupon#20 + DI + beads 
Sample notes	 
Experiment notes	DI Deionised water, 25 mm diameter. 70 mm total depth of water, 10 mm gap, with PE beads
Operator	M Rides
Sample density	1.000 g/cm^3
Results file name	AR1756
Run number	1 
Results directory	D:\ARG2 rheometer\Test files\Southampton University P Stoodley May2012
Experiment was run on	15/03/2013 14:43:45

Procedure name	Flow procedure
Procedure notes	

Step name	Conditioning Step 1
Step notes	
Perform step	No
Initial temperature	20.0 C
Wait for correct temperature	Yes
Do set temperature	Yes
Wait for normal force	No
Perform pre-shear	No
Perform equilibration	Yes
Equilibration duration	0:00:30 hh:mm:ss
Wait for zero velocity	No
Control normal force	Uses current instrument settings
Purge gas only	No

Step name	Continuous ramp step 1
Step notes	
Perform step	No

Step name	Peak hold step
Step notes	
Perform step	Yes
Ramp type	Peak hold
Controlled variable	velocity 50.00 rad/s
Duration	0:01:00 hh:mm:ss
Delay time	0:00:01 hh:mm:ss
Temperature	20.0 C
Wait for temperature	No
Motor mode	auto 

Step name	Continuous ramp step 2
Step notes	
Perform step	No

Step name	Post-Experiment Step
Step notes	
Perform step	Yes
Do set temperature	Yes
Temperature	20.0 C
Set temperature system idle	No

Geometry name	25mm ETC plastic plate Southampton
Geometry notes	25 mm diameter parallel plastic plate with ETC rod
Geometry material	Other
Parallel plate diameter	25.00 mm
gap	10000 micro m
Gap offset	0 micro m
Geometry inertia	0.4094 micro N.m.s^2
Geometry compliance	2.020E-3 rad/N.m
Gap temperature compensation	0 micro m/C
Gap temperature compensation enabled	No
Shear rate factor	1.250 
Shear stress factor	3.259E5 1/m^3
Measurement system factor	2.608E5 1/m^3
Fluid density factor	1.278E-10 m^5
Normal force factor	4074 1/m^2
Backoff distance	5000 micro m
Approximate sample volume	4.91 ml

Sample compression	linear 
Compression distance	1000.0 micro m
Compression velocity	50.0 micro m/s
Fine velocity	500.0 micro m/s
Coarse velocity	6000.0 micro m/s
Other velocity	6000.0 micro m/s
Current temperature system	Peltier plate
Temperature control	Enabled 
Purge gas only	No
Temperature calibration	Peltier plate - 0.6 micro m/C
	Water bath - 0 micro m/C
	Torsion oven - plate - 0 micro m/C
	Torsion oven - solid sample - 0 micro m/C
	Peltier concentric cylinders - 0 micro m/C
	None - 0 micro m/C
	Stress relaxation - 0 micro m/C
	Current temperature system - 0 micro m/C
Cooling water temperature	15.0 C
Cooling water range	6.0 C
Bearing friction correction	Yes
Bearing friction	0.261 micro N.m/(rad/s)
Bearing offset	0 micro N.m
Temperature system span and offset	Peltier plate - span 1.0000 , offset 0 C
	Water bath - span 1.0000 , offset 0 C
	Torsion oven - plate - span 1.0000 , offset 0 C
	Torsion oven - solid sample - span 1.0000 , offset 0 C
	Peltier concentric cylinders - span 1.0000 , offset 0 C
	None - span 1.0000 , offset 0 C
	Stress relaxation - span 1.0000 , offset 0 C
	Current temperature system - span 1.0000 , offset 0 C
Bearing mapping type	precision 
Number of mapping iterations	2
Instrument type (MType)	AR-G2
Firmware version	  8.29  27/10/09
Configuration version (CnfVer)	301
Parameter version (PrmVer)	301
PCB Number	*NOT_SET*
IP address	192.168.1.2
Software version	V5.8.0
Windows version	Windows XP 5.1 (Service Pack 2)
Instrument inertia	21.14 micro N.m.s^2
Auto increment run number	Yes
Prompt for file name at start of run	Yes
Auto save results file	Yes
Results file storage	Consecutive steps of same type to 1 file 
Temperature tolerance	0.2 C
Temperature duration	0:00:10 hh:mm:ss
Wait for temperature even if OK	Yes
Gap tolerance	4 micro m
Gap duration	0:00:02 hh:mm:ss
Override wait for gap	No
Velocity tolerance	0.1000 rad/s
Zero speed after pre-shear	Leave as is 
Zero normal force before run	No
Zero timer before run	Before pre-shear 
Non-equilibrium minimum velocity	1.000E-4 rad/s
Zero strain at the start of each flow step	Yes
Inertia correction	Yes
Collect negative shear rate data if stress is positive	Yes
Collect all points	No
Display flow point graph during run	Yes
Store flow point graph with results	Yes
Store images to the results for flow steps	Yes
Creep zero displacement	Yes
Store images to the results for creep steps	Yes
Standard creep image store frequency	10 s
Repeated creep image store frequency in repeats	10 
Display oscillation waveform graph during run	Yes
Store oscillation waveform graph with results	Yes
Display strain control tries during run	Yes
Store strain control tries with results	Yes
Store images to the results for oscillation steps	Yes
Stress relaxation zero displacement	Yes
Store images to the results for stress relaxation steps	Yes
Flow torque limit	10.00 micro N.m
Flow velocity limit	1.000E-3 rad/s
Oscillation torque limit	5.00 micro N.m
Oscillation displacement limit	1.00E-5 rad
Oscillation raw phase limit	170.0 degrees
Oscillation minimum normal force limit	0.1000 N
Oscillation maximum normal force limit	50.00 N
Flow velocity tolerance	1.00 %
Oscillation torque tolerance	1.00 %
Oscillation displacement tolerance	1.00 %
Oscillation velocity tolerance	1.00 %
Temperature tolerance	1.0 C

Peak hold step

time	velocity	torque	gap	temperature	normal force	time global	shear stress	shear rate	viscosity	normal stress	displacement	normal stress coefficient	strain	% strain	1/temperature	time	time global
s	rad/s	micro N.m	micro m	C	N	s	Pa	1/s	Pa.s	Pa	rad	Pa.s^2			1/K	min	min

1.0000	49.35	-1780.8	10000	20.0	0.1256	1.000	-580.5	61.69	-9.410	511.7	25.7990	0.1345	32.249	3224.9	3.411E-3	0.0	0.0
1.9960	49.99	35.393	10000	20.0	0.2384	1.996	11.54	62.49	0.1846	971.3	75.2489	0.2487	94.061	9406.1	3.411E-3	0.0	0.0
3.0080	50.00	35.611	10000	20.0	0.1475	3.008	11.61	62.49	0.1857	601.0	125.1040	0.1539	156.38	15638	3.411E-3	0.1	0.1
3.9960	50.00	35.525	10000	20.0	0.1607	3.996	11.58	62.50	0.1853	654.7	175.5970	0.1676	219.50	21950	3.411E-3	0.1	0.1
5.0000	50.00	37.050	10000	20.0	0.1507	5.000	12.08	62.50	0.1932	614.2	225.6250	0.1572	282.03	28203	3.411E-3	0.1	0.1
5.9960	50.00	37.244	10000	20.0	0.1514	5.996	12.14	62.50	0.1942	616.7	275.8770	0.1579	344.85	34485	3.411E-3	0.1	0.1
6.9960	50.00	36.711	10000	20.0	0.1554	6.996	11.97	62.50	0.1915	633.2	326.1330	0.1621	407.67	40767	3.411E-3	0.1	0.1
8.0000	50.00	36.127	10000	20.0	0.1528	8.000	11.78	62.50	0.1884	622.5	376.7930	0.1594	470.99	47099	3.411E-3	0.1	0.1
8.9960	50.00	36.272	10000	20.0	0.1497	8.996	11.82	62.50	0.1892	610.1	426.6870	0.1562	533.36	53336	3.411E-3	0.1	0.1
9.9960	50.00	36.410	10000	20.0	0.1499	9.996	11.87	62.50	0.1899	610.9	477.5350	0.1564	596.92	59692	3.411E-3	0.2	0.2
10.996	50.00	36.531	10000	20.0	0.1522	10.996	11.91	62.50	0.1905	620.0	527.4550	0.1587	659.32	65932	3.411E-3	0.2	0.2
12.000	50.00	36.848	10000	20.0	0.1505	12.000	12.01	62.50	0.1922	613.4	577.4480	0.1570	721.81	72181	3.411E-3	0.2	0.2
13.000	50.00	36.794	10000	20.0	0.1538	13.000	11.99	62.50	0.1919	626.6	627.9160	0.1604	784.90	78490	3.411E-3	0.2	0.2
13.992	50.00	36.705	10000	20.0	0.1503	13.992	11.96	62.50	0.1914	612.5	677.9890	0.1568	847.49	84749	3.411E-3	0.2	0.2
14.996	50.00	35.955	10000	20.0	0.1526	14.996	11.72	62.50	0.1875	621.6	728.2800	0.1591	910.35	91035	3.411E-3	0.2	0.2
16.000	50.00	36.253	10000	20.0	0.1489	16.000	11.82	62.50	0.1891	606.8	778.5780	0.1553	973.22	97322	3.411E-3	0.3	0.3
16.992	50.00	36.102	10000	20.0	0.1538	16.992	11.77	62.50	0.1883	626.6	829.0290	0.1604	1036.3	1.0363E5	3.411E-3	0.3	0.3
18.000	50.00	36.199	10000	20.0	0.1534	18.000	11.80	62.50	0.1888	625.0	879.1700	0.1600	1099.0	1.0990E5	3.411E-3	0.3	0.3
18.992	50.00	36.252	10000	20.0	0.1534	18.992	11.82	62.50	0.1891	625.0	930.0530	0.1600	1162.6	1.1626E5	3.411E-3	0.3	0.3
19.992	50.00	36.066	10000	20.0	0.1512	19.992	11.76	62.50	0.1881	615.9	979.8800	0.1577	1224.9	1.2249E5	3.411E-3	0.3	0.3
20.992	50.00	36.142	10000	20.0	0.1510	20.992	11.78	62.50	0.1885	615.0	1030.3000	0.1574	1287.9	1.2879E5	3.411E-3	0.3	0.3
21.996	50.00	35.832	10000	20.0	0.1507	21.996	11.68	62.50	0.1869	614.2	1080.4000	0.1572	1350.5	1.3505E5	3.411E-3	0.4	0.4
23.000	50.00	35.710	10000	20.0	0.1493	23.000	11.64	62.50	0.1862	608.4	1130.9100	0.1558	1413.6	1.4136E5	3.411E-3	0.4	0.4
23.992	50.00	35.847	10000	20.0	0.1520	23.992	11.68	62.50	0.1869	619.2	1180.9301	0.1585	1476.2	1.4762E5	3.411E-3	0.4	0.4
24.992	50.00	35.643	10000	20.0	0.1520	24.992	11.62	62.50	0.1859	619.2	1231.1700	0.1585	1539.0	1.5390E5	3.411E-3	0.4	0.4
25.992	50.00	35.945	10000	20.0	0.1520	25.992	11.72	62.50	0.1875	619.2	1281.8700	0.1585	1602.3	1.6023E5	3.411E-3	0.4	0.4
27.004	50.00	35.546	10000	20.0	0.1495	27.004	11.59	62.50	0.1854	609.2	1331.6899	0.1560	1664.6	1.6646E5	3.411E-3	0.5	0.5
28.000	50.00	35.426	10000	20.0	0.1479	28.000	11.55	62.50	0.1848	602.6	1382.0000	0.1543	1727.5	1.7275E5	3.411E-3	0.5	0.5
28.992	50.00	35.827	10000	20.0	0.1542	28.992	11.68	62.50	0.1868	628.3	1432.7300	0.1608	1790.9	1.7909E5	3.411E-3	0.5	0.5
29.992	50.00	35.679	10000	20.0	0.1510	29.992	11.63	62.50	0.1861	615.0	1482.3199	0.1574	1852.9	1.8529E5	3.411E-3	0.5	0.5
30.992	50.00	35.407	10000	20.0	0.1505	30.992	11.54	62.50	0.1847	613.4	1532.7300	0.1570	1915.9	1.9159E5	3.411E-3	0.5	0.5
31.996	50.00	35.094	10000	20.0	0.1493	31.996	11.44	62.50	0.1830	608.4	1582.7800	0.1558	1978.5	1.9785E5	3.411E-3	0.5	0.5
33.000	50.00	35.403	10000	20.0	0.1520	33.000	11.54	62.50	0.1846	619.2	1633.0699	0.1585	2041.3	2.0413E5	3.411E-3	0.6	0.6
33.992	50.00	35.819	10000	20.0	0.1510	33.992	11.68	62.50	0.1868	615.0	1683.3000	0.1575	2104.1	2.1041E5	3.411E-3	0.6	0.6
34.996	50.00	35.763	10000	20.0	0.1501	34.996	11.66	62.50	0.1865	611.7	1733.5800	0.1566	2167.0	2.1670E5	3.411E-3	0.6	0.6
35.992	50.00	35.635	10000	20.0	0.1475	35.992	11.62	62.50	0.1858	601.0	1783.8400	0.1539	2229.8	2.2298E5	3.411E-3	0.6	0.6
36.996	50.00	35.400	10000	20.0	0.1495	36.996	11.54	62.50	0.1846	609.2	1834.3000	0.1560	2292.9	2.2929E5	3.411E-3	0.6	0.6
38.036	50.00	35.871	10000	20.0	0.1512	38.036	11.69	62.50	0.1871	615.9	1884.7300	0.1577	2355.9	2.3559E5	3.411E-3	0.6	0.6
38.996	50.00	35.745	10000	20.0	0.1544	38.996	11.65	62.50	0.1864	629.1	1934.6500	0.1610	2418.3	2.4183E5	3.411E-3	0.6	0.6
39.996	50.00	35.805	10000	20.0	0.1493	39.996	11.67	62.50	0.1867	608.4	1985.7100	0.1558	2482.1	2.4821E5	3.411E-3	0.7	0.7
41.000	50.00	35.708	10000	20.0	0.1556	41.000	11.64	62.50	0.1862	634.0	2036.4700	0.1623	2545.6	2.5456E5	3.411E-3	0.7	0.7
41.992	50.00	35.104	10000	20.0	0.1516	41.992	11.44	62.50	0.1831	617.5	2085.4600	0.1581	2606.8	2.6068E5	3.411E-3	0.7	0.7
43.000	50.00	35.683	10000	20.0	0.1518	43.000	11.63	62.50	0.1861	618.3	2135.7200	0.1583	2669.7	2.6697E5	3.411E-3	0.7	0.7
43.992	50.00	35.968	10000	20.0	0.1505	43.992	11.72	62.50	0.1876	613.4	2185.9600	0.1570	2732.5	2.7325E5	3.411E-3	0.7	0.7
44.992	50.00	35.658	10000	20.0	0.1544	44.992	11.62	62.50	0.1860	629.1	2236.5000	0.1610	2795.6	2.7956E5	3.411E-3	0.7	0.7
45.992	50.00	35.840	10000	20.0	0.1507	45.992	11.68	62.50	0.1869	614.2	2286.5000	0.1572	2858.1	2.8581E5	3.411E-3	0.8	0.8
46.992	50.00	35.492	10000	20.0	0.1507	46.992	11.57	62.50	0.1851	614.2	2336.7700	0.1572	2921.0	2.9210E5	3.411E-3	0.8	0.8
48.000	50.00	35.631	10000	20.0	0.1497	48.000	11.61	62.50	0.1858	610.1	2387.0200	0.1562	2983.8	2.9838E5	3.411E-3	0.8	0.8
48.992	50.00	35.484	10000	20.0	0.1495	48.992	11.57	62.50	0.1851	609.2	2437.6699	0.1560	3047.1	3.0471E5	3.411E-3	0.8	0.8
49.992	50.00	35.934	10000	20.0	0.1501	49.992	11.71	62.50	0.1874	611.7	2487.5701	0.1566	3109.5	3.1095E5	3.411E-3	0.8	0.8
50.992	50.00	36.026	10000	20.0	0.1497	50.992	11.74	62.50	0.1879	610.1	2537.8201	0.1562	3172.3	3.1723E5	3.411E-3	0.8	0.8
51.992	50.00	36.031	10000	20.0	0.1534	51.992	11.74	62.50	0.1879	625.0	2588.1001	0.1600	3235.1	3.2351E5	3.411E-3	0.9	0.9
53.000	50.00	35.723	10000	20.0	0.1568	53.000	11.64	62.50	0.1863	639.0	2638.6699	0.1636	3298.3	3.2983E5	3.411E-3	0.9	0.9
53.996	50.00	35.987	10000	20.0	0.1510	53.996	11.73	62.50	0.1877	615.0	2688.8799	0.1574	3361.1	3.3611E5	3.411E-3	0.9	0.9
54.992	50.00	35.449	10000	20.0	0.1522	54.992	11.55	62.50	0.1849	620.0	2738.8999	0.1587	3423.6	3.4236E5	3.411E-3	0.9	0.9
55.996	50.00	35.730	10000	20.0	0.1581	55.996	11.65	62.50	0.1863	644.0	2789.2000	0.1649	3486.5	3.4865E5	3.411E-3	0.9	0.9
56.992	50.00	35.801	10000	20.0	0.1578	56.992	11.67	62.50	0.1867	643.1	2839.4099	0.1646	3549.3	3.5493E5	3.411E-3	0.9	0.9
58.016	50.00	35.460	10000	20.0	0.1522	58.016	11.56	62.50	0.1849	620.0	2889.6899	0.1587	3612.1	3.6121E5	3.411E-3	1.0	1.0
58.996	50.00	35.658	10000	20.0	0.1578	58.996	11.62	62.50	0.1860	643.1	2939.9700	0.1646	3675.0	3.6750E5	3.411E-3	1.0	1.0
59.992	50.00	35.441	10000	20.0	0.1491	59.992	11.55	62.50	0.1848	607.6	2990.4700	0.1555	3738.1	3.7381E5	3.411E-3	1.0	1.0

